Vigilancia Tecnológica

Fe?based composite was developed with improved biocompatibility for biodegradable implants. Fe?based composite incorporating 10%HA/??TCP is fabricated using solid?state manufacturing. High?pressure torsion (HPT consolidation is utilized, resulting in crack?free structures even after 1 rotation. Increasing HPT rotations leads to enhanced density and decreased lath thickness. Improved mechanical properties and modulated degradation rate suggest potential for thinner, smaller implant designs.Day?by?day biodegradable alloys and composites are getting more attention. Besides their competing material properties with traditional permanent implants, their harmless degradation in the body eliminates the need for a second surgery to remove the implant. Beyond other biodegradable materials such as Mg and Zn, Fe is known with high strength with low degradation rate. However there is still need to improve its biocompatibility. Herein, a Fe?based composite is developed via solid?state manufacturing route. 10% HA/??TCP is selected as an additive which is a biocompatible ceramic material and the powder mix is ball?milled. Afterward, the powders are consolidated via high?pressure torsion (HPT) with 1–5–10 revolutions at room temperature. Crack?free structures are obtained even after 1?HTP rotation. Fe is in lamellar form around HA??TCP particles. With the increase of HPT rotation numbers, lath thickness decreased. After 10 HPT rotations, 24% enhancement in density is observed that points to a more condensed structure. Transmission electron microscopy observations show significant grain refinement after 1?HPT rotation, and Fe grain size remains constant (?300?nm) up to 10 turns. Ultimate tensile strength increases while degradation rate decreases after 5?HPT rotations. This study provides the potential of enhanced Fe?based biomaterials for thinner and smaller implant designs.